i was in my chem lab today and had a test tube that contained a solution of Ammonium Chloride (NH4Cl) and Sodium Cobaltinitrite (NaCo(N02)6 and instead of disposing of it i decided to pour a little bit of 18 molar sulfuric acid to it (Horrible Idea!!!). anyways i cant figure out what kind of gas the reaction produced but i think it might have been nitrous oxide because i guess i breathed some in and i almost passed out and my heart started racing. it was a really scary experience.
some of the HCl escaped from the solution because the reaction is exothermic.
So you probably breathed in some HCl vapor - not pleasant.
I have no idea what the reaction is with H2SO4 on the Cobalt complex (if any).
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